ASTM C1674-23 PDF
Standard Test Method for Flexural Strength of Advanced Ceramics with Engineered Porosity (Honeycomb Cellular Channels) at Ambient Temperatures
Standard Test Method for Flexural Strength of Advanced Ceramics with Engineered Porosity (Honeycomb Cellular Channels) at Ambient Temperatures
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 25
- Дата публикации:
- 1 июня 2023 г.
- Издание:
- C1674
- ICS:
- 81.060.30
SIGNIFICANCE AND USE 5.1 This test method is used to determine the mechanical properties in flexure of engineered ceramic components with multiple longitudinal hollow channels, commonly described as “honeycomb” channel architectures. The components generally have 30 % or more porosity and the cross-sectional dimensions of the honeycomb channels are on the order of 1 mm or greater. 5.2 The experimental data and calculated strength values from this test method are used for material and structural development, product characterization, design data, quality control, and engineering/production specifications. Note 1: Flexure testing is the preferred method for determining the nominal “tensile fracture” strength of these components, as compared to a compression (crushing) test. A nominal tensile strength is required, because these materials commonly fail in tension under thermal gradient stresses. A true tensile test is difficult to perform on these honeycomb specimens because of gripping and alignment challenges. 5.3 The mechanical properties determined by this test method are both material and architecture dependent, because the mechanical response and strength of the porous test specimens are determined by a combination of inherent material properties and microstructure and the architecture of the channel porosity [porosity fraction/relative density, channel geometry (shape, dimensions, cell wall thickness, etc.), anisotropy and uniformity, etc.] in the specimen. Comparison of test data must consider both differences in material/composition properties as well as differences in channel porosity architecture between individual specimens and differences between and within specimen lots. 5.4 Test Method A is a user-defined specimen geometry with a choice of four-point or three-point flexure testing geometries. It is not possible to define a single fixed specimen geometry for flexure testing of honeycombs, because of the wide range of honeycomb architectures and cell sizes and consid... SCOPE 1.1 This test method covers the determination of the flexural strength (modulus of rupture in bending) at ambient conditions of advanced ceramic structures with 2-dimensional honeycomb channel architectures. 1.2 The test method is focused on engineered ceramic components with longitudinal hollow channels, commonly called “honeycomb” channels (see Fig. 1). The components generally have 30 % or more porosity and the cross-sectional dimensions of the honeycomb channels are on the order of 1 mm or greater. Ceramics with these honeycomb structures are used in a wide range of applications (catalytic conversion supports (1),2 high temperature filters (2, 3), combustion burner plates (4), energy absorption and damping (5), etc.). The honeycomb ceramics can be made in a range of ceramic compositions—alumina, cordierite, zirconia, spinel, mullite, silicon carbide, silicon nitride, graphite, and carbon. The components are produced in a variety of geometries (blocks, plates, cylinders, rods, rings). FIG. 1 General Schematics of Typical Honeycomb Ceramic Structures 1.3 The test method describes two test specimen geometries for determining the flexural strength (modulus of rupture) for a porous honeycomb ceramic test specimen (see Fig. 2): FIG. 2 Flexure Loading Configurations L = Outer Span Length (for Test Method A, L = User defined; for Test Method B, L = 90 mm) Note 1: 4-Point-1/4 Loading for Test Methods A1 and B. Note 2: 3-Point Loading for Test Method A2. 1.3.1 Test Method A—A 4-point or 3-point bending test with user-defined specimen geometries, and 1.3.2 Test Method B—A 4-point-1/4 point bending test with a defined rectangular specimen geometry (13 mm × 25 mm × > 116 mm) and a 90 mm outer support span geometry suitable for cordierite and silicon carbide honeycombs with small cell sizes. 1.4 The test specimens are stressed to failure and the breaking force value, specimen and cell dimensions, and loa...
Abstract
Overview
ASTM C1674-23 is the international standard test method developed by ASTM International for determining the flexural strength of advanced ceramics with engineered porosity, specifically those with honeycomb cellular channels, at ambient temperatures. This standard applies to ceramic components featuring multiple longitudinal hollow channels, often referred to as honeycomb channel architectures, with 30% or more porosity and channel dimensions of approximately 1 mm or greater.
The standard helps laboratories, manufacturers, and product designers evaluate key mechanical properties in flexure (modulus of rupture in bending) of such engineered ceramics across various geometries and compositions. The data gathered through this method is vital for material and structural development, product characterization, design validation, and ongoing quality control.
Key Topics
- Honeycomb Ceramics Characterization: The method targets ceramics with engineered, controlled macroporosity (notably, “honeycomb” architectures). Applications demand understanding both material composition and channel architecture (shape, cell wall thickness, anisotropy, etc.) for accurate mechanical assessment.
- Test Methods:
- Test Method A: User-defined specimen geometry allowing flexibility for specimens with varying honeycomb architectures. Offers either four-point or three-point flexure testing configurations.
- Test Method B: Specifies a standardized rectangular specimen and a four-point-¼ point loading geometry, ideal for certain ceramics like cordierite and silicon carbide honeycombs with small cell sizes.
- Measurement Approaches: The procedure enables calculation of three types of flexural strength - nominal beam strength, wall fracture strength, and honeycomb structure strength - providing a comprehensive understanding based on specimen geometry, channel size, and porosity.
- Material and Architectural Dependence: The results account for the combined effects of intrinsic material properties and engineered pore geometry, making this standard particularly suitable for comparing different honeycomb ceramic materials and designs.
Applications
Advanced ceramics with engineered honeycomb porosity are essential in numerous industrial applications that demand a combination of lightweight structure, controlled permeability, and reliable strength. Typical uses include:
- Catalytic Converter Supports: Honeycomb ceramics act as substrates that maximize surface area while supporting catalysts in automotive and industrial emission control systems.
- High-Temperature Filters: Used in filtration systems for hot gases and particulates, these ceramics offer thermal stability and resistance to aggressive environments.
- Combustion Burner Plates: Their high thermal shock resistance and designed porosity suit combustion environments for energy generation and processing.
- Energy Absorption and Damping: Components engineered for controlled crash-energy management or vibration damping in automotive, aerospace, and industrial applications.
The flexural strength data referenced from ASTM C1674-23 supports product development, comparative material selection, and routine quality assurance, while also guiding design requirements for end users.
Related Standards
Several ASTM standards complement or are referenced in ASTM C1674-23 for comprehensive mechanical characterization of advanced ceramics:
- ASTM C1161: Standard Test Method for Flexural Strength of Advanced Ceramics at Ambient Temperature.
- ASTM C373: Methods for Determination of Water Absorption and Related Properties of Ceramic Tiles.
- ASTM C1198 / C1259: Test Methods for Dynamic Young's Modulus and Poisson’s Ratio (by sonic resonance and impulse excitation).
- ASTM C1239: Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Ceramics.
- ASTM C1525: Test Method for Determination of Thermal Shock Resistance.
- ASTM D2344 / D2344M: Short-beam Strength of Polymer Matrix Composite Materials.
- ASTM E4, E6, E337, E691, E177: Various standards for mechanical test apparatus calibration, humidity measurements, and precision/bias reporting.
By adhering to ASTM C1674-23 and the associated guidance, organizations can efficiently test, compare, and verify the flexural performance of honeycomb-structured advanced ceramics for critical applications.
Keywords: ASTM C1674, flexural strength, honeycomb ceramics, advanced ceramics, engineered porosity, ceramic materials testing, product development, automotive ceramics, quality control, porous ceramics, channel architecture.
Технические детали
- Технический комитет
- C28 - Advanced Ceramics
- SKU
- ASTM C1674-23
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