ASTM D5550-23 PDF
Standard Test Method for Specific Gravity of Soil Solids by Gas Pycnometer
Standard Test Method for Specific Gravity of Soil Solids by Gas Pycnometer
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 7
- Дата публикации:
- 1 января 2023 г.
- Издание:
- D5550
- ICS:
- 13.080.10
SIGNIFICANCE AND USE 5.1 The specific gravity value is used in many phase relation equations to determine relative volumes of particle, water, and gas mixtures. 5.2 The term soil particle typically refers to a naturally occurring mineral grain that is not readily soluble in water. Therefore, the specific gravity of soils that contain extraneous matter (such as cement, lime, and the like) or water-soluble material (such as salt) must be corrected for the precipitate that forms on the test specimen after drying. If the precipitate has a specific gravity less than the parent soil grains, the uncorrected test result will be too low. If the precipitate has a higher specific gravity, then the uncorrected test value will be too high. 5.3 Heating during drying may diagenetically alter the structure of some clay minerals.3 Therefore caution should be exercised if the mineral composition of a clay test specimen is going to be determined after drying. It is possible to dry the test specimen at a lower temperature. However, the effect on water content4 and hence specific gravity should be investigated. In addition, some materials other than clay may be affected by drying at 110°C, such as gypsum, soils containing organics, fly ash containing residual coal, island sands. Test Method D2216 includes recommendations for drying gypsum using a lower temperature, such as 60°C. Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors. SCOPE 1.1 This test method covers the determination of the specific gravity of soil solids by means of a gas pycnometer. Particle size is limited by the dimensions of the test specimen container of the particular pycnometer being used. 1.2 Test Method D854 may be used instead of or in conjunction with this test method for performing specific gravity tests on soils. Note that Test Method D854 does not require the specialized test apparatus needed by this test method. However, Test Method D854 may not be used if the test specimen contains matter that can readily dissolve in water, whereas this test method does not have that limitation. 1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026. 1.3.1 For purposes of comparing a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal or significant digits in the specified limits. 1.3.2 The procedures used to specify how data are collected/recorded and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design. 1.4 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. 1.4.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs. The converted slug unit is not given, un...
Abstract
Overview
ASTM D5550-23 is the recognized standard test method for determining the specific gravity of soil solids using a gas pycnometer. Issued by ASTM International, this standard establishes a reliable procedure for accurate measurement of soil particle density-a critical parameter in geotechnical engineering, soil science, and construction quality control. The test is applicable to soil samples containing materials that may dissolve in water, offering a key advantage over water pycnometer methods. ASTM D5550-23 supports improved precision in phase relationship calculations for soil, water, and gas mixtures.
Key Topics
- Specific Gravity Measurement: Focuses on the determination of the specific gravity of soil solids, defined as the ratio of the mass of soil to the mass of an equal volume of distilled water at 4°C.
- Gas Pycnometer Use: The method employs a gas pycnometer, which measures specimen volume based on gas displacement. Helium is commonly used for accuracy, but other inert gases can be acceptable per equipment specifications.
- Sample Preparation and Handling:
- Oven-drying at 110°C (or lower as needed for certain materials per related standards)
- Use of desiccators to prevent reabsorption of moisture prior to analysis
- Sample pulverization as necessary for size consistency
- Correction for Soluble Components: Procedures address correction of specific gravity for soils containing water-soluble materials (e.g., salts), preventing biased results due to precipitation after drying.
- Precision and Repeatability: The standard describes proper calibration, equipment requirements, and quality control procedures to ensure measurement accuracy.
- Reporting Requirements: Clear guidance on data recording-including specimen identification, test conditions, mass, volume, and correction factors-is provided for traceable, repeatable results.
Applications
The ASTM D5550-23 test method serves industries and professionals engaged in:
- Geotechnical Engineering: Supports soil classification, compaction control, and calculation of phase relationships necessary for foundation and earthwork engineering.
- Soil Science and Environmental Assessment: Essential for examining mineral composition, porosity, and interactions in natural and amended soils.
- Construction Quality Assurance: Used to verify soil material properties in accordance with project specifications and ensure consistency across laboratory and field samples.
- Research and Academic Study: Facilitates advanced investigation into soil microstructure and mineralogy, where accurate density metrics are required.
The method is suitable for all non-soluble soil mineral grains, and is particularly valuable when water pycnometer methods are unsuitable due to the presence of water-soluble components.
Related Standards
Several ASTM standards are referenced within ASTM D5550-23 for terminology, apparatus, and related test methods:
- ASTM D653 - Terminology relating to soil, rock, and fluids
- ASTM D854 - Test methods for specific gravity of soil solids by water pycnometer (alternative when no soluble matter is present)
- ASTM D2216 - Determination of water (moisture) content of soil and rock by mass
- ASTM D3740 - Practice for agency competence in soil and rock testing
- ASTM D4318 - Determination of liquid and plastic limits, and plasticity index of soils
- ASTM D4542 - Pore water extraction and determination of soluble salt content
- ASTM D4753 - Guidelines for balances and standard masses
- ASTM D6026 - Practice for significant digits and data reporting in geotechnical data
Keywords: ASTM D5550, specific gravity of soil, gas pycnometer, soil solids, geotechnical testing, soil phase relationships, soil density, laboratory soil testing, water content, soil salinity correction.
By adhering to ASTM D5550-23, laboratories and professionals ensure high-precision and industry-accepted soil specific gravity measurements, essential for quality-driven soil analysis and engineering design.
Технические детали
- Технический комитет
- D18 - Soil and Rock
- SKU
- ASTM D5550-23
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