ISO 10070:2019
Metallic powders — Determination of envelope-specific surface area from measurements of the permeability to air of a powder bed under steady-state flow conditions
Metallic powders — Determination of envelope-specific surface area from measurements of the permeability to air of a powder bed under steady-state flow conditions
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 18
- Дата публикации:
- 4 декабря 2019 г.
- Издание:
- ISO IS 10070 edition 2 version 1
- ICS:
- 77.160
This document specifies a method of measuring the air permeability and the porosity of a packed bed of metal powder, and of deriving therefrom the value of the envelope-specific surface area. The permeability is determined under steady-state flow conditions, using a laminar flow of air at a pressure near atmospheric. This document does not include the measurement of permeability by a constant volume method. Several different methods have been proposed for this determination, and several test devices are available commercially. They give similar, reproducible results, provided that the general instructions given in this document are respected, and the test parameters are identical. This document does not specify a particular commercial test device and corresponding test procedure. However, for the convenience of the user, an informative annex has been included (see Annex A) which is intended to give some practical information on three specific methods: — the Lea and Nurse method, involving a test device which can be built in a laboratory (see A.1); — the Zhang Ruifu method, using a similar test device (see A.2); — the Gooden and Smith method, involving a test device which can be built in a laboratory but for which a commercial test device also exists. (Two types of commercial test device exist; one of these is no longer available for purchase, but is still being used, see A.3.) These methods are given as examples only. Other test devices available in various countries are acceptable within the scope of this document. This testing method is applicable to all metallic powders, including powders for hardmetals, up to 1 000 µm in diameter, but it is generally used for particles having diameters between 0,2 µm and 75,0 µm. It is not intended to be used for powders composed of particles whose shape is far from equiaxial, i.e. flakes or fibres, unless specifically agreed upon between the parties concerned. This testing method is not applicable to mixtures of different metallic powders or powders containing binders or lubricant. If the powder contains agglomerates, the measured surface area can be affected by the degree of agglomeration. If the powder is subjected to a de-agglomeration treatment (see Annex B), the method used is to be agreed upon between the parties concerned.
Abstract
Overview
ISO 10070:2019 specifies a laboratory method to determine the envelope-specific surface area of metallic powders from measurements of the permeability to air of a packed powder bed under steady‑state (constant pressure drop) laminar flow conditions near atmospheric pressure. The standard applies to metallic powders (including hardmetal powders) up to 1 000 µm in diameter, though it is typically used for particles between 0.2 µm and 75.0 µm. ISO 10070:2019 is device‑agnostic - it describes principles, calculations and general procedure and includes an informative annex (Annex A) with practical examples of specific test methods (Lea & Nurse, Zhang Ruifu, Gooden & Smith).
Key topics and technical requirements
- Permeametry principle: Measure volume flow rate and pressure drop of dry air across a packed powder bed and calculate permeability using Darcy’s law.
- Surface area derivation: Convert permeability and permeable porosity into an envelope‑specific surface area using the Kozeny‑Carman relation and the Carman‑Arnell modification (accounts for slip flow).
- When to use which formula: Use the Carman‑Arnell formulation when volume‑specific surface area is > 10 m‑1 (mean particle size < ~6 µm) because slip flow becomes significant; Kozeny‑Carman may be used for coarser powders by agreement.
- Test conditions: Steady‑state laminar flow, air at near atmospheric pressure; constant volume (variable pressure) methods are excluded.
- Scope limits: Not intended for non‑equiaxial particles (flakes, fibres) unless agreed; not applicable to powder mixtures, powders containing binders or lubricants; agglomeration affects results and de‑agglomeration procedures (Annex B) must be agreed between parties.
- Device flexibility: The standard does not mandate commercial equipment; Annex A gives examples of lab-built and commercial devices for guidance.
- Reporting: Requires reporting of permeability, porosity, test parameters and converted equivalent sphere diameter when relevant.
Applications and users
ISO 10070:2019 is used by:
- Powder manufacturers and suppliers for quality control and specification of metallic powders
- Powder metallurgy and additive manufacturing R&D teams evaluating particle characteristics
- QC/analytical laboratories performing surface area and porosity testing
- Instrument and test‑equipment manufacturers validating permeametry devices Practical uses include characterizing powders for sintering, compaction, flowability assessments, and converting permeability data into envelope‑surface metrics used in process control and material specifications.
Related standards
- ISO 3954 (Powders for powder metallurgical purposes - Sampling) is referenced as a normative document.
Note: Envelope‑specific surface area from permeametry differs from total surface area measured by gas adsorption methods; the two are complementary for powder characterization.
Keywords: ISO 10070, metallic powders, envelope-specific surface area, permeability to air, powder bed, permeametry, Kozeny‑Carman, Carman‑Arnell, porosity, powder metallurgy.
Технические детали
- Технический комитет
- ISO/TC 119/SC 2 - Sampling and testing methods for powders (including powders for hardmetals)
- SKU
- ISO 10070:2019
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