ISO 13736:2021
Determination of flash point — Abel closed-cup method
Determination of flash point — Abel closed-cup method
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 24
- Дата публикации:
- 31 марта 2021 г.
- Издание:
- ISO IS 13736 edition 4 version 1
- ICS:
- 75.080
This document specifies a method for the determination of the manual and automated closed cup flash point of combustible liquids having flash points between –30,0 °C to 75,0 °C. However, the precision given for this method is only valid for flash points in the range −8,5 °C to 75,0 °C. This document is not applicable to water-borne paints. NOTE 1 Water borne paints can be tested using ISO 3679[1]. NOTE 2 See 9.1 for the importance of this test in avoiding loss of volatile materials. NOTE 3 Liquids containing halogenated compounds can give anomalous results. NOTE 4 The thermometer specified for the manual apparatus limits the upper test temperature to 70,0 °C. NOTE 5 See 13.1 for more specific information related to precision.
Abstract
Overview
ISO 13736:2021 - "Determination of flash point - Abel closed‑cup method" specifies the manual and automated Abel closed‑cup test for determining the flash point of combustible liquids. The method covers liquids with flash points between −30.0 °C and 75.0 °C, with stated precision valid for −8.5 °C to 75.0 °C. The standard defines apparatus design, sampling, test procedure, temperature measurement, pressure correction and reporting rules required to obtain reproducible closed‑cup flash point results.
Key topics and technical requirements
- Scope & limitations
- Applicable to combustible liquids in the stated temperature range.
- Not applicable to water‑borne paints (see ISO 3679).
- Liquids with halogenated compounds can give anomalous results.
- Manual thermometer limits upper manual test temperature to 70.0 °C.
- Principle
- Test portion is heated under continuous stirring in the Abel test cup. An ignition source is applied at intervals; the lowest temperature producing ignition across the liquid surface is recorded as the flash point.
- Apparatus and verification
- Detailed apparatus dimensions and requirements in Annex A.
- Thermometer installation and specifications in Annex B and Annex C; digital contact thermometers allowed if they meet accuracy and response requirements.
- Annex D (normative) covers apparatus verification using CRMs and secondary working standards.
- Measurement & controls
- Barometer with absolute pressure reading accurate to 0.5 kPa; flash point adjusted for atmospheric pressure deviations from 101.3 kPa.
- Timing device accuracy better than 5%.
- Cleaning solvents, coolants (ethylene glycol/water, glycerol/water or silicone oil), lubricants and appropriate ignitor/pilot gases are specified for correct operation.
- Precision and reporting
- Precision statements updated in line with ISO 4259‑1; full reporting requirements and details are provided in Clauses 11–14 and Annex E.
Practical applications
- Regulatory classification for shipping, storage and handling of flammable/combustible liquids.
- Quality control in petroleum, fuel and chemical manufacturing to detect volatile fractions or process consistency.
- Safety assessments used by HSE, transport authorities and emergency responders to determine storage/transport requirements.
- Laboratory testing for certification, supplier verification and preliminary investigation of unknown materials.
Who should use ISO 13736:2021
- Petroleum and fuel laboratories, chemical manufacturers, testing & calibration labs, regulatory agencies, transport & storage safety teams, and industrial hygiene professionals performing flash point testing using the Abel closed‑cup method.
Related standards
- ISO 3679 (water‑borne paints testing)
- ISO 3170 / ISO 3171 (sampling petroleum liquids)
- ISO 15528 (paints/varnishes sampling)
- ISO 4259‑1 (precision definitions)
- ISO/TR 29662 (guidance on flash point testing)
Keywords: ISO 13736:2021, Abel closed‑cup method, flash point determination, closed cup flash point, combustible liquids, flash point testing, test apparatus, flash point precision.
Технические детали
- Технический комитет
- ISO/TC 28 - Petroleum and related products, fuels and lubricants from natural or synthetic sources
- SKU
- ISO 13736:2021
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Стандарты, упомянутые в описании
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