ISO 15301:2001

Name: ISO 15301:2001 — Animal and vegetable fats and oils — Determination of sediment in crude fats and oils — Centrifuge method
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Animal and vegetable fats and oils — Determination of sediment in crude fats and oils — Centrifuge method

Название (английский):

ISO 15301:2001

Animal and vegetable fats and oils — Determination of sediment in crude fats and oils — Centrifuge method

Статус документа:: Действующий
Формат:: Электронный (PDF)
Количество страниц:: 9
Дата публикации:: 20 сентября 2001 г.
Издание:: ISO IS 15301 edition 1 version 1
ICS:: 67.200.10

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Описание (английский):

La présente Norme internationale spécifie une méthode pour la détermination de la teneur en sédiment dans des corps gras bruts susceptibles d'être séparés par la force centrifuge. Cette méthode est applicable aux corps gras bruts, ainsi qu'aux corps gras obtenus par extraction et/ou pression, dont la teneur en sédiment est comprise entre 0,03 ml par 100 g et 15 ml par 100 g. Cette méthode n'est pas applicable aux corps gras non liquides à une température de 20°C.

Abstract

Похожие стандарты

Стандарты, упомянутые в описании

Overview

ISO 15301:2001 specifies a rapid centrifuge method for the determination of sediment in crude animal and vegetable fats and oils. The method measures the volume of insoluble material that can be separated by centrifugal force and is applicable to crude oils (including oils from extraction and crushing) with sediment contents from 0.03 ml/100 g to 15 ml/100 g. It is not applicable to fats that are solid at 20 °C.

Key topics and technical requirements

Scope and definition: Sediment is the centrifugally separable portion of insoluble matter (e.g., phospholipids, impurities, particulate dirt) collected as an unclear layer at the bottom of the tube.

Sample preparation: Prepare test samples following ISO 661 and equilibrate to 20 °C ±2 to 5 °C. Redisperse any settled material before testing.

Apparatus:

100 ml pear- or cone-shaped glass centrifuge tubes with stoppers.
Oil-resistant buckets and a centrifuge capable of delivering 700–800 × g at the narrow part of the tube (see Annex A for frequency calculation).
Balance with 0.1 g readability.

Procedure:

Weigh empty tubes, add 100 ml of test sample, re-weigh, centrifuge for 1 h at the specified relative acceleration.
Read sediment volume: up to 1.5 ml with fine resolution (document specifies small-volume reading), volumes >1.5 ml to 0.5 ml resolution.
Record centrifuge speed/acceleration (or swing diameter), and temperature before and after centrifuging.

Calculation and reporting:

Sediment content w (ml/100 g) is calculated using the formula provided in the standard (based on sediment volume V and tube masses).
Report mean of two tubes to the nearest 1 ml/100 g and include all test conditions in the report.

Precision:

Repeatability and reproducibility limits are provided (e.g., for sediment <1 ml/100 g: r = 0.1 ml/100 g, R = 0.7 ml/100 g; for 1–3 ml/100 g: r = 0.2, R = 1.0).

Applications - who uses this standard

Quality control laboratories in edible oil processing, refining and cold-pressed oil production for routine sediment testing.

Trade and inspection bodies (traders, import/export inspectors) for rapid assessment of crude oil quality.

Research and development groups comparing centrifuge results to longer methods.

Regulatory agencies using standardized methods for compliance and labeling.

Practical benefits include fast turnaround versus the 96 h settling method (ISO 15301 shows strong correlation and is suitable for rapid control when sediment exceeds ~0.5 ml/100 g).

Related standards

ISO 661 - Preparation of test sample

ISO 5555 - Sampling of fats and oils

ISO 5725-2 - Precision (repeatability and reproducibility) of measurement methods

Keywords: ISO 15301:2001, sediment determination, centrifuge method, fats and oils, crude oil sediment, sediment content, centrifuge tubes, repeatability, reproducibility.

ISO 15301:2001

Abstract

Похожие стандарты

Overview

Key topics and technical requirements

Applications - who uses this standard

Related standards

Технические детали

ISO 6618:1997

Petroleum products and lubricants — Determination of acid or base number — Colour-indicator titration method

BS EN ISO 15301:2001

Animal and vegetable fats and oils. Determination of sediment in crude fats and oils. Centrifuge method.

ISO 5555:2001

Animal and vegetable fats and oils — Sampling

ISO 5725-2:1994

Accuracy (trueness and precision) of measurement methods and results — Part 2: Basic method for the determina…