ISO 19581:2025
Measurement of radioactivity — Gamma emitting radionuclides — Rapid screening method using scintillation detector gamma-ray spectrometry
Measurement of radioactivity — Gamma emitting radionuclides — Rapid screening method using scintillation detector gamma-ray spectrometry
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 22
- Дата публикации:
- 24 сентября 2025 г.
- Издание:
- ISO IS 19581 edition 2 version 1
- ICS:
- 17.240
This document specifies a screening test method to quantify rapidly the activity concentration of gamma-emitting radionuclides, such as 131I, 132Te, 134Cs and 137Cs, in solid or liquid test samples using gamma-ray spectrometry with lower resolution scintillation detectors as compared with the HPGe detectors (see IEC 61563[7]). This test method can be used for the measurement of any potentially contaminated environmental matrices (including soil), food and feed samples as well as industrial materials or products that have been properly conditioned[8]. Sample preparation techniques used in the screening method are not specified in this document, since special sample preparation techniques other than simple machining (cutting, grinding, etc.) should not be required. Although the sampling procedure is of utmost importance in the case of the measurement of radioactivity in samples, it is out of scope of this document; other International Standards for sampling procedures that can be used in combination with this document are available (see References [ REF Reference_ref_12 \r \h 9 08D0C9EA79F9BACE118C8200AA004BA90B0200000008000000110000005200650066006500720065006E00630065005F007200650066005F00310032000000 ] [10] [11] [12] [13] [14]). The test method applies to the measurement of gamma-emitting radionuclides such as 131I, 134Cs and 137Cs. Using sample sizes of 0,5 l to 1,0 l in a Marinelli beaker and a counting time of 5 min to 20 min, decision threshold of 10 Bq·kg−1 can be achievable using a commercially available scintillation spectrometer [e.g. thallium activated sodium iodide (NaI(Tl)) spectrometer 2” ϕ × 2” (50,8 mm Ø x 50,8 mm) detector size, 7 % resolution (FWHM) at 662 keV, 30 mm lead shield thickness]. This test method also can be performed in a “makeshift” laboratory or even outside a testing laboratory on samples directly measured in the field where they were collected. During a nuclear or radiological emergency, this test method enables a rapid measurement of the activity concentration of potentially contaminated samples to check against operational intervention levels (OILs) set up by decision makers that would trigger a predetermined emergency response to reduce existing radiation risks[2]. Due to the uncertainty associated with the results obtained with this test method, test samples requiring more accurate test results can be measured using high purity germanium (HPGe) detectors gamma-ray spectrometry in a testing laboratory, following appropriate preparation of the test samples[15][16]. This document does not contain criteria to establish the activity concentration of OILs.
Abstract
Overview
ISO 19581:2025 - Measurement of radioactivity - Gamma emitting radionuclides - Rapid screening method using scintillation detector gamma‑ray spectrometry - specifies a fast screening test method for quantifying activity concentrations of gamma‑emitting radionuclides (for example 131I, 132Te, 134Cs, 137Cs) in solids and liquids using lower‑resolution scintillation detector gamma‑ray spectrometry (e.g., NaI(Tl)). The standard is intended for rapid field or makeshift‑laboratory screening during routine monitoring and nuclear or radiological emergencies, enabling comparisons against operational intervention levels (OILs).
Key topics and technical requirements
- Scope and intent: Rapid screening of environmental matrices, food, feed and industrial materials using scintillation gamma‑ray spectrometers rather than HPGe systems.
- Detector examples: Practical reference to commercially available NaI(Tl) scintillation spectrometers (e.g., 2" Ø × 2", ~7% FWHM at 662 keV) and recommended shielding (example: 30 mm lead).
- Sample geometry and timing: Typical sample volumes of 0.5–1.0 L in a Marinelli beaker with counting times of 5–20 minutes are covered.
- Performance targets: A decision threshold around 10 Bq·kg−1 can be achievable with the example setup, subject to sample matrix and conditions.
- Calibration and validation: Procedures for energy calibration, detection efficiency calibration, use of reference and check sources, and validation of the screening level are included.
- Procedure limits: The document does not specify detailed sample preparation beyond simple machining (cutting, grinding) and does not cover sampling procedures or define OIL criteria; it recommends following existing sampling standards and, for higher accuracy, subsequent measurement using HPGe detectors.
- Reporting: Requirements for test reports and uncertainty considerations are included to ensure fit‑for‑purpose results.
Applications
- Emergency response: Rapid screening of soil, food, water, milk and other matrices to assess if activity concentrations exceed OILs and to support immediate protective action decisions.
- Environmental monitoring: Preliminary surveys and triage measurements where rapid turnaround is more important than laboratory precision.
- Field campaigns & makeshift labs: On‑site measurements at collection points or temporary facilities when HPGe access is limited.
- Industrial screening: Quick checks of materials and products for gamma contamination.
Who should use this standard
- Radiation protection laboratories, emergency response teams, environmental monitoring agencies, food safety authorities, and field technicians conducting rapid gamma‑screening using scintillation spectrometers.
Related standards
- IEC 61563 (gamma‑ray spectrometry system characteristics and HPGe reference)
- Relevant ISO/Codex/IAEA documents on sampling, OILs and radionuclide screening (referenced within ISO 19581:2025).
Keywords: ISO 19581:2025, gamma‑ray spectrometry, scintillation detector, NaI(Tl), rapid screening, 137Cs, 134Cs, 131I, emergency response, Marinelli beaker, detection efficiency, calibration.
Технические детали
- Технический комитет
- ISO/TC 85/SC 2 - Radiological protection
- SKU
- ISO 19581:2025
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