ISO 19668:2017

Name: ISO 19668:2017 — Surface chemical analysis — X-ray photoelectron spectroscopy — Estimating and reporting detection limits for elements in homogeneous materials
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Surface chemical analysis — X-ray photoelectron spectroscopy — Estimating and reporting detection limits for elements in homogeneous materials

Название (английский):

ISO 19668:2017

Surface chemical analysis — X-ray photoelectron spectroscopy — Estimating and reporting detection limits for elements in homogeneous materials

Статус документа:: Действующий
Формат:: Электронный (PDF)
Количество страниц:: 24
Дата публикации:: 14 августа 2017 г.
Издание:: ISO IS 19668 edition 1 version 1
ICS:: 71.040.40

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Описание (английский):

ISO 19668:2017 specifies a procedure by which elemental detection limits in X-ray photoelectron spectroscopy (XPS) can be estimated from data for a particular sample in common analytical situations and reported. This document is applicable to homogeneous materials and is not applicable if the depth distribution of elements is inhomogeneous within the information depth of the technique.

Abstract

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Overview

ISO 19668:2017 - "Surface chemical analysis - X‑ray photoelectron spectroscopy (XPS) - Estimating and reporting detection limits for elements in homogeneous materials" provides a standardized, practical procedure to estimate and report elemental detection limits from XPS measurements. The standard is specifically applicable to homogeneous materials and is not intended where the element depth distribution is inhomogeneous within the XPS information depth.

Keywords: ISO 19668:2017, XPS, X‑ray photoelectron spectroscopy, detection limits, surface chemical analysis, homogeneous materials.

Key topics and requirements

Purpose: Calculate elemental detection limits from actual XPS data and report them consistently.

Applicability: Only for homogeneous samples; inapplicable for inhomogeneous depth distributions.

Required data: knowledge of elemental relative sensitivity factors (RSFs) (or use of AMRSFs with transmission corrections), summed intensities for detected elements, and the binding energy (BE) or kinetic energy (KE) of the target photoelectron peak (known to ~10 eV).

Spectra requirements: spectrum covering the expected BE of the specified element; at least 20 background data points free of sharp spectral features.

Composition guidance: if the specified element is detected, its concentration should be <10 at.% (preferably <1 at.%).

Noise and background: procedures for calculating background noise and standard deviation from counts or from a background fit are specified.

Detection limit calculation: step‑by‑step method to derive minimal detectable summed intensity and convert it to an elemental detection limit (atomic percent or areal/thickness equivalents).

Reporting: clear requirements on how to report detection limits and related parameters.

Uncertainty: informative Annex A describes uncertainties (typical uncertainty of calculated XPS detection limits is about 10–25%).

Supporting material: Annex B (definitions), Annex C (examples), Annex D (conversion methods).

Practical applications and users

ISO 19668:2017 is useful for:

XPS analysts and surface scientists who must quantify low‑level elemental presence or demonstrate non‑detection with confidence.

Quality control and failure‑analysis labs performing surface contamination checks or thin film characterization.

Instrument manufacturers and method developers establishing or validating detection limit performance.

Regulatory or certification processes that require standardized reporting of XPS detection limits.

Practical benefits:

Provides a reproducible approach to quantify what “not detected” means under specific measurement conditions.

Enables planning of acquisition time and instrument settings to achieve a target detection limit.

Improves comparability and traceability of XPS results across labs.

ISO 19668:2017

Abstract

Похожие стандарты

Overview

Key topics and requirements

Practical applications and users

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