ISO 3679:2022
Determination of flash point – Method for flash no-flash and flash point by small scale closed cup tester
Determination of flash point – Method for flash no-flash and flash point by small scale closed cup tester
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 27
- Дата публикации:
- 4 ноября 2022 г.
- Издание:
- ISO IS 3679 edition 5 version 1
- ICS:
- 75.080
This document describes three procedures (A, B and C) covering determinations of flash no-flash and flash point. Rapid equilibrium procedures A and B are applicable to flash no-flash and flash point tests of paints, including water-borne paints, varnishes, binders for paints and varnishes, adhesives, solvents, petroleum products including aviation turbine, diesel and kerosene fuels, fatty acid methyl esters and related products over the temperature range –30 °C to 300 °C. The rapid equilibrium procedures are used to determine whether a product will or will not flash at a specified temperature (flash no-flash procedure A) or the flash point of a sample (procedure B). When used in conjunction with the flash detector (A.1.6), this document is also suitable to determine the flash point of fatty acid methyl esters (FAME). The validity of the precision is given in Table 2. Non-equilibrium procedure C is applicable to petroleum products including aviation turbine, diesel and kerosine fuels, and related petroleum products, over the temperature range –20 °C to 300 °C. The non-equilibrium procedure is automated to determine the flash point. Precision has been determined over the range 40 °C to 135 °C. For specifications and regulations, procedures A or B are routinely used (see 10.1.1).
Abstract
Overview
ISO 3679:2022 specifies a small scale closed cup tester method for determination of flash point and flash no-flash results. The standard defines three procedures:
- Procedure A - rapid equilibrium flash no-flash (pass/fail at a specified temperature)
- Procedure B - rapid equilibrium flash point determination
- Procedure C - automated non‑equilibrium flash point determination
The method covers paints (including water-borne), varnishes, adhesives, solvents, petroleum products (including aviation turbine, diesel and kerosene fuels), fatty acid methyl esters (FAME / biodiesel) and related products over wide temperature ranges (procedures A/B: −30 °C to 300 °C; procedure C: −20 °C to 300 °C). The apparatus supports small test portions (2 ml or 4 ml) and can be made portable for on‑site testing.
Key topics and requirements
- Test procedures: Clear instructions for flash no-flash (A), flash point measurement (B) and automated flash point (C).
- Applicability: Specific product families and temperature ranges; suitability of FAME with a flash detector (A.1.6).
- Apparatus: Small scale closed cup tester design, verification and maintenance (Annex A, Annex B).
- Sampling & sample handling: Guidance for liquids, solids/semi‑solids and samples containing water (Clauses 8–9).
- Verification & calibration: Requirements for apparatus verification, temperature measuring device specs (Annex E) and use of cup inserts (Annex C).
- Precision and uncertainty: Precision statements (Clause 13), with procedure C precision assessed in the 40 °C to 135 °C range; repeatability and reproducibility criteria are described.
- Safety & limitations: Warnings about unstable, decomposable or explosive materials and method-dependent nature of flash point results.
Practical applications
- Regulatory classification for flammability, storage, transport and handling of fuels, solvents and paints.
- Quality control in fuel production, biodiesel (FAME) testing and paint/varnish manufacture.
- Rapid on‑site screening (flash no-flash) to decide if a product will ignite at a given temperature.
- Preliminary screening prior to more detailed compositional analysis.
Who should use ISO 3679:2022
- Test laboratories and QC teams in petroleum and paint industries
- Biodiesel and fuel producers assessing FAME flash behavior
- Safety, compliance and regulatory professionals responsible for classification and storage rules
- Manufacturers needing portable, small-sample flash point testing
Related standards
- ISO 1516, ISO 1523 (other closed cup equilibrium methods)
- ISO/TR 29662 (guidance on flash point testing and interpretation)
- Sampling and reference material standards cited in ISO 3679 (e.g., ISO 3170, ISO 3171, ISO 15528, ISO Guide 35)
Keywords: ISO 3679:2022, flash point, flash no‑flash, small scale closed cup tester, FAME, biodiesel, petroleum fuels, paints, on‑site testing, procedure A B C.
Технические детали
- Технический комитет
- ISO/TC 28 - Petroleum and related products, fuels and lubricants from natural or synthetic sources
- SKU
- ISO 3679:2022
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