ASTM D2697-22
Standard Test Method for Volume Nonvolatile Matter in Clear or Pigmented Coatings
Standard Test Method for Volume Nonvolatile Matter in Clear or Pigmented Coatings
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 4
- Дата публикации:
- 1 июля 2022 г.
- Издание:
- D2697
- ICS:
- 87.040
SIGNIFICANCE AND USE 4.1 This test method is intended to provide a measure of the volume of dry coating obtainable from a given volume of liquid coating. This value is useful for comparing the coverage (square feet of surface covered at a specified dry film thickness per unit volume) obtainable with different coating products. 4.2 For various reasons the value obtained may not be equal to that predicted from simple additivity of the weights and volumes of the raw materials in a formulation. One reason is that the volume occupied by a solution of resin in solvent may be the same, greater, or less than the total volume of the separate ingredients: such contraction or expansion in resin solutions is governed by a number of factors, one of which is the extent and direction of spread between solubility parameters of the resin and solvent. 4.3 The spatial configuration of the pigment particles and the degree to which the spaces between the pigment particles are filled with the binder also affect the volume of a dry coating formulation. Above the critical pigment volume concentration, the apparent volume of the dry film is significantly greater than theoretical due to the increase in unfilled voids between pigment particles. The use of volume nonvolatile matter values in such instances should be carefully considered as the increased volume is largely due to air trapped in these voids. SCOPE 1.1 This test method is believed to be applicable to the determination of the volume of nonvolatile matter of a variety of coatings. An interlaboratory study to establish the precision of this test method included a water-reducible exterior latex paint and three automotive coatings that included a solvent-reducible primer surfacer, water reducible primer surfacer, water reducible enamel topcoat, and acrylic dispersion lacquer topcoat. Earlier collaborative studies included a gloss enamel, a flat wall paint, a gloss house enamel, an industrial baking enamel, an interior latex paint, and an exterior latex paint. This method does not apply to radiation curable materials or pigmented coatings. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Abstract
Overview
ASTM D2697-22: Standard Test Method for Volume Nonvolatile Matter in Clear or Pigmented Coatings is an internationally recognized standard developed by ASTM International. This test method is essential in the paint and coatings industry for determining the volume of nonvolatile matter-often referred to as solids by volume-in a wide range of clear or pigmented coatings. The method quantifies the volume of dry coating achievable from a defined volume of liquid coating, providing critical information for evaluating product coverage and assessing different coating formulations.
The standard is widely adopted by manufacturers, formulators, and users of architectural, automotive, and industrial coatings to ensure product performance and compliance with industry requirements.
Key Topics
- Nonvolatile Content Measurement: Defines procedures for accurately measuring the volume percent of nonvolatile matter (solids) in coatings after drying using gravimetric and volumetric techniques.
- Applicable Coating Types: Encompasses a variety of coating products including water-reducible latex paints, solvent-reducible primers, enamels, lacquers, and baking enamels. Not applicable for radiation-curable materials or some highly pigmented coatings.
- Testing Methodology: Utilizes a stainless steel disk or aluminum tube to apply, dry, and weigh the coating to determine changes in mass and volume. Immersion in liquids of known density (such as water or mineral spirits) is used to calculate volume displacement.
- Coverage Determination: Results enable users to calculate theoretical coverage of a coating per unit volume at a specified thickness, improving product selection and project planning.
- Precision and Interpretation: Includes guidance on repeatability and reproducibility to assure test reliability across laboratories. Notes limitations due to formulation variables such as resin-solvent interactions or pigment volume concentration.
Applications
- Comparing Coating Products: The test results allow specifiers and end users to compare the effective coverage of different coatings, especially when selecting products for large projects where material efficiency impacts cost and performance.
- Formulation Development: Coating manufacturers use this standard to optimize their products for solids content, directly influencing coverage, finish characteristics, and application properties.
- Quality Control: Routine use of ASTM D2697-22 supports quality assurance programs by enabling consistent assessment of batch-to-batch product uniformity regarding nonvolatile volume.
- Regulatory and Specification Compliance: Ensures coatings meet industry standards and contractual requirements for solids content and coverage, which are often specified in project documents, technical data sheets, and environmental regulations.
- Research and Development: Supports the evaluation of new binder systems, pigment technologies, and innovative coating solutions by providing a reproducible metric for coating efficiency.
Related Standards
For comprehensive coatings evaluation and quality control, ASTM D2697-22 is often used in conjunction with these related ASTM standards:
- ASTM D1475: Test Method for Density of Liquid Coatings, Inks, and Related Products
- ASTM D2369: Test Method for Volatile Content of Coatings
- ASTM D3925: Practice for Sampling Liquid Paints and Related Pigmented Coatings
- ASTM D5403: Test Methods for Volatile Content of Radiation Curable Materials
Conclusion
ASTM D2697-22 is a critical standard for determining volume nonvolatile matter in clear or pigmented coatings. Accurate measurement of solids by volume is fundamental to predicting coating performance and ensuring compliance with specifications. Regular implementation of this standard enables manufacturers, quality control labs, and end users to select, formulate, and apply coatings with confidence-helping maximize material efficiency and project outcomes.
Технические детали
- Технический комитет
- D01 - Paint and Related Coatings, Materials, and Applications
- SKU
- ASTM D2697-22
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