EN ISO 14577-1:2026
Metallic materials - Instrumented indentation test for hardness and materials parameters - Part 1: Test method (ISO 14577-1:2026)
Metallic materials - Instrumented indentation test for hardness and materials parameters - Part 1: Test method (ISO 14577-1:2026)
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 50
- Дата публикации:
- 24 июня 2026 г.
- Издание:
- CEN EN 14577 edition 2 version 1
- ICS:
- 77.040.10
This document specifies the method of instrumented indentation test for determination of hardness and other materials parameters for the following three ranges: macro range: 2 N ≤ F ≤ 30 kN; micro range: 2 N > F; h > 0,2 µm; nano range: h ≤ 0,2 µm. For the nano range, the mechanical deformation strongly depends on the real shape of indenter tip and the calculated material parameters are significantly influenced by the contact area function of the indenter used in the testing machine. Therefore, careful calibration of both instrument and indenter shape is required in order to achieve an acceptable reproducibility of the materials parameters determined with different machines. The macro and micro ranges are distinguished by the test forces in relation to the indentation depth. Attention is drawn to the fact that the micro range has an upper limit given by the test force (2 N) and a lower limit given by the indentation depth of 0,2 µm. The determination of hardness and other material parameters is given in the normative Annex A. At high contact pressures, damage to the indenter is possible. For test pieces with very high hardness and modulus of elasticity, permanent indenter deformation can occur and can be detected using suitable reference materials. Indentations that result in damage or permanent deformation of the indenter are excluded from the scope of this test method. This test method can also be applied to thin metallic and non-metallic coatings and non-metallic materials. In this case, it is recommended that the specifications in the relevant standards be taken into account (see also 7.3 and ISO 14577-4). The analysis methods of this standard assume that materials behave like ideal materials. Any deviation (internal stress, pile-up, sink-in, densification, phase transitions, cracks) will result in additional uncertainties. This becomes especially important if comparisons shall be done to material parameters, obtained with other methods.
Abstract
Overview
EN ISO 14577-1:2026 defines the instrumented indentation test method for measuring hardness and other material parameters of metallic materials. Published by CEN and harmonized with ISO 14577-1:2026, this standard is essential for mechanical testing across a wide range of force and depth scales, including macro, micro, and nano ranges. It provides a structured approach for achieving accurate and reproducible hardness measurements using force and depth data, offering significant value for material characterization and quality control in industrial, research, and engineering applications.
Key Topics
-
Indentation Ranges:
- Macro range: Test force between 2 N and 30 kN
- Micro range: Force below 2 N, indentation depth above 0.2 µm
- Nano range: Indentation depth at or below 0.2 µm
-
Test Methodology:
- Detailed procedures for preparing test pieces and calibrating equipment
- Instrument calibration and indenter shape are crucial, especially for nano-indentation, to minimize measurement uncertainties
- Both force-controlled and displacement-controlled methods are included to address a range of testing needs
-
Uncertainty and Calibration:
- Emphasizes the need for uncertainty evaluation according to recognized measurement guidelines (ISO/IEC Guide 98-3)
- Reproducibility depends on accurate calibration of both the indentation instrument and the indenter tip area function
-
Applicability to Coatings and Non-Metallics:
- The standard is suitable for testing thin metallic and non-metallic coatings, as well as certain non-metallic materials, provided relevant specifications and specific standards (such as ISO 14577-4) are observed
-
Limitations:
- Damage or permanent deformation of the indenter from extremely hard materials is outside the standard’s recommended practices
- Assumes ideal material behavior; deviations such as internal stress, cracks, or phase transitions may increase uncertainty in results
Applications
EN ISO 14577-1:2026 is widely used in industries and research fields where the mechanical properties of materials must be measured with precision and reliability, including:
- Metallurgy and Metalworking: For quality control of raw materials, semi-finished, and finished metal products through hardness and modulus determination
- Surface Engineering: Assessment of thin films, metallic coatings, and surface treatments
- Advanced Materials Research: Characterization of new alloys, composites, and nanostructured materials
- Product Development and Validation: Ensures materials meet specified performance criteria in automotive, aerospace, and manufacturing sectors
- Calibration Laboratories: Standardizes test procedures and uncertainty calculation for traceable results
By following this instrumented indentation testing standard, organizations can achieve:
- Improved measurement reproducibility and comparability across labs and testing equipment
- Detailed understanding of depth-dependent mechanical properties
- Better product and process optimization based on reliable hardness and materials parameters
Related Standards
For comprehensive implementation of instrumented indentation methods and measurement of material parameters, the following standards should also be consulted:
- ISO 14577-2: Verification and calibration of testing machines for instrumented indentation
- ISO 14577-3: Calibration of reference blocks
- ISO 14577-4: Test method for metallic and non-metallic coatings, crucial for coatings analysis
- ISO 14577-5: Linear elastic dynamic instrumented indentation testing (DIIT)
- ISO/IEC Guide 98-3: Uncertainty of measurement - Guide to the expression of uncertainty in measurement (GUM)
By integrating EN ISO 14577-1:2026 with these related documents, laboratories and testing facilities can strengthen their mechanical testing protocols, enhance data reliability, and meet international quality compliance requirements.
Keywords: EN ISO 14577-1:2026, instrumented indentation test, hardness test, mechanical properties, metallic materials, nanoindentation, microhardness, material parameters, calibration, measurement uncertainty, coatings, material testing standards.
Технические детали
- Технический комитет
- ECISS/TC 101 - Test methods for steel (other than chemical analysis)
- SKU
- EN ISO 14577-1:2026
Похожие стандарты
Стандарты, упомянутые в описании
ISO 14577-1:2026
ДействующийMetallic materials — Instrumented indentation test for hardness and materials parameters — Part 1: Test method
Overview ISO 14577-1:2026 defines the standardized instrumented indentation test method for assessing hardness and other material parameters of metallic materials. This internationally recognized sta…
ISO 14577-4:2016
ДействующийMetallic materials — Instrumented indentation test for hardness and materials parameters — Part 4: Test metho…
Overview ISO 14577-4:2016 defines an instrumented indentation test method for determining hardness and material parameters of metallic and non‑metallic coatings, optimized for the nano/micro range an…
BS EN ISO 14577-2:2026
ДействующийMetallic materials. Instrumented indentation test for hardness and materials parameters. Verification and cal…
BS EN ISO 14577-3:2026
ДействующийMetallic materials. Instrumented indentation test for hardness and materials parameters. Calibration of refer…
ISO 14577-5:2022
ДействующийMetallic materials — Instrumented indentation test for hardness and materials parameters — Part 5: Linear ela…
Overview ISO 14577-5:2022 - "Metallic materials - Instrumented indentation test for hardness and materials parameters - Part 5: Linear elastic dynamic instrumented indentation testing (DIIT)" specifi…