EN ISO 10070:2019 PDF
Metallic powders - Determination of envelope-specific surface area from measurements of the permeability to air of a powder bed under steady-state flow conditions (ISO 10070:2019)
Metallic powders - Determination of envelope-specific surface area from measurements of the permeability to air of a powder bed under steady-state flow conditions (ISO 10070:2019)
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 26
- Дата публикации:
- 18 декабря 2019 г.
- Издание:
- CEN EN 10070 edition 1 version 1
- ICS:
- 77.160
This document specifies a method of measuring the air permeability and the porosity of a packed bed of metal powder, and of deriving therefrom the value of the envelope-specific surface area. The permeability is determined under steady-state flow conditions, using a laminar flow of air at a pressure near atmospheric. This document does not include the measurement of permeability by a constant volume method. Several different methods have been proposed for this determination, and several test devices are available commercially. They give similar, reproducible results, provided that the general instructions given in this document are respected, and the test parameters are identical. This document does not specify a particular commercial test device and corresponding test procedure. However, for the convenience of the user, an informative annex has been included (see Annex A) which is intended to give some practical information on three specific methods: — the Lea and Nurse method, involving a test device which can be built in a laboratory (see A.1); — the Zhang Ruifu method, using a similar test device (see A.2); — the Gooden and Smith method, involving a test device which can be built in a laboratory but for which a commercial test device also exists. (Two types of commercial test device exist; one of these is no longer available for purchase, but is still being used, see A.3.) These methods are given as examples only. Other test devices available in various countries are acceptable within the scope of this document. This testing method is applicable to all metallic powders, including powders for hardmetals, up to 1 000 µm in diameter, but it is generally used for particles having diameters between 0,2 µm and 75,0 µm. It is not intended to be used for powders composed of particles whose shape is far from equiaxial, i.e. flakes or fibres, unless specifically agreed upon between the parties concerned. This testing method is not applicable to mixtures of different metallic powders or powders containing binders or lubricant. If the powder contains agglomerates, the measured surface area can be affected by the degree of agglomeration. If the powder is subjected to a de-agglomeration treatment (see Annex B), the method used is to be agreed upon between the parties concerned.
Abstract
Overview
EN ISO 10070:2019 - Metallic powders: Determination of envelope-specific surface area from measurements of the permeability to air of a powder bed under steady‑state flow conditions - defines a permeametry method to measure the air permeability, porosity, and derive the envelope‑specific surface area of metallic powders. The method uses a laminar air flow at near‑atmospheric pressure under steady‑state (constant pressure drop) conditions. This standard is intended for powder metallurgy applications and is published by CEN/ISO.
Key topics and technical requirements
- Measured quantities: air permeability of a packed powder bed, porosity, envelope‑specific surface area and (optionally) equivalent sphere diameter.
- Flow conditions: steady‑state laminar flow (constant pressure drop); constant volume methods are excluded.
- Applicable powders: all metallic powders (including hardmetals) up to 1 000 µm diameter, commonly used for particles 0.2–75.0 µm. Not intended for highly non‑equiaxial shapes (flakes, fibres) unless agreed by parties.
- Limitations: not applicable to mixtures of different metallic powders or powders containing binders or lubricants. Measured surface area is the envelope surface (excludes closed/blind pores) and can differ from gas‑adsorption total surface area.
- Formulations and models: the standard discusses permeability–porosity relationships (e.g., Carman‑Arnell and Kozeny‑Carman formulations) and the assumptions that affect calculated surface area.
- Annexes and methods: informative Annex A describes practical implementations - Lea & Nurse, Zhang Ruifu and Gooden & Smith methods (Gooden & Smith now includes an automated/commercial device in the 2019 edition). Annex B covers de‑agglomeration treatments and their effect on results.
- Reporting: specifies test preparation, packed bed formation, measurement procedure, expression of results and required test report details. ISO 3954 (sampling) is referenced for sample selection.
Applications and users
- Who uses it: powder manufacturers, quality control laboratories, research & development teams in powder metallurgy, sintered component producers, and suppliers of powder testing equipment. It is also relevant for additive manufacturing and hardmetal production where powder surface area and flow/packing behavior affect processing.
- Practical uses: characterizing powder flow/permeability for process control, comparing batches, converting envelope surface area to equivalent particle size for specification, verifying de‑agglomeration effects, and calibrating permeametry instruments.
Related standards
- ISO 3954 (Powders for powder metallurgical purposes - Sampling) - normative reference cited in EN ISO 10070:2019.
Keywords: EN ISO 10070:2019, metallic powders, envelope-specific surface area, permeability to air, powder bed, steady-state flow, permeametry, Carman-Kozeny, de-agglomeration, powder metallurgy.
Технические детали
- Технический комитет
- CEN/SS M11 - Powder metallurgy
- SKU
- EN ISO 10070:2019
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