IEC TS 62607-6-7:2023 PDF
Nanomanufacturing - Key control characteristics - Part 6-7: Graphene - Sheet resistance: van der Pauw method
Nanomanufacturing - Key control characteristics - Part 6-7: Graphene - Sheet resistance: van der Pauw method
- Статус документа:
- Действующий
- Формат:
- Электронный (PDF)
- Количество страниц:
- 27
- Дата публикации:
- 7 июня 2023 г.
- Издание:
- IEC TS 62607 edition 1 version 1
- ICS:
- 07.120
IEC TS 62607-6-7:2023 establishes a method to determine the key control characteristics sheet resistance RS [measured in ohm per square (Ω/sq)], by the van der Pauw method, vdP. The sheet resistance RS is derived by measurements of four-terminal electrical resistance performed on four electrical contacts placed on the boundary of the planar sample and calculated with a mathematical expression involving the two resistance measurements. The measurement range for RS of the graphene samples with the method described in this document goes from 10−2 Ω/sq to 104 Ω/sq. The method is applicable for CVD graphene provided it is transferred to quartz substrates or other insulating materials (quartz, SiO2 on Si), as well as graphene grown from silicon carbide. The method is complementary to the in-line four-point-probe method (4PP, IEC 62607-6-8) for what concerns the measurement of the sheet resistance and can be applied when it is possible to reliably place contacts on the sample boundary, avoiding the sample being scratched by the 4PP. The outcome of the van der Pauw method is independent of the contact position provided the sample is uniform, which is typically not true for graphene at this stage. This document considers the case of samples with non-strictly uniform conductivity distribution and suggests a way to consider the sample inhomogeneity as a component of the uncertainty on RS.
Abstract
Overview
IEC TS 62607-6-7:2023 - Nanomanufacturing: Graphene - Sheet resistance: van der Pauw method defines a standardized procedure to measure the sheet resistance (RS, in ohm per square Ω/sq) of graphene using the van der Pauw (vdP) technique. The Technical Specification covers four‑terminal resistance measurements made with four electrical contacts on the sample perimeter, the calculation of RS from two resistance measurements, and guidance on uncertainty evaluation and sample non‑uniformity. The method applies to CVD graphene transferred to insulating substrates (quartz, SiO2 on Si) and graphene grown on silicon carbide, with an effective measurement range from 10−2 Ω/sq to 10^4 Ω/sq.
Key Topics
- Measurement principle: Four‑terminal vdP measurements (two resistance configurations) with contacts on the sample boundary and mathematical computation of RS.
- Measurement range: Valid for RS between 10−2 and 10^4 Ω/sq.
- Sample applicability: CVD graphene on quartz or other insulating supports, and graphene from silicon carbide.
- Contact independence & uniformity: vdP is independent of contact position for uniform samples; the standard addresses realistic graphene inhomogeneity and recommends treating non‑uniformity as an uncertainty component.
- Measurement procedure: Protocols for contact placement, instrument calibration, measurement settings, and recording of environmental conditions (temperature, relative humidity).
- Uncertainty and data analysis: Methods to compute RS, apply corrections, and express combined uncertainty including sample inhomogeneity.
- Practical considerations: Avoiding sample damage (e.g., versus in‑line four‑point‑probe 4PP), use of commercial vdP fixtures, and recommended reporting of results.
Applications / Who Should Use It
This Technical Specification is aimed at laboratories and organizations involved in graphene metrology, quality control, and device fabrication:
- Nanomanufacturers and process engineers validating sheet resistance of CVD or SiC graphene films.
- R&D teams developing graphene‑based electronics, sensors, and transparent conductors.
- Test and calibration labs establishing traceable RS measurements and uncertainty budgets.
- Quality assurance in roll‑to‑roll production where non‑destructive edge contact measurement is preferred to 4PP. Using IEC TS 62607-6-7:2023 helps ensure reproducible, comparable RS data for product specifications and process control.
Related Standards
- IEC TS 62607-6-8 (in‑line four‑point‑probe method) - complementary method for sheet resistance measurement.
- Annex C of IEC TS 62607-6-7 lists additional standards and references relevant to sheet resistance metrology and measurement best practices.
Keywords: IEC TS 62607-6-7:2023, van der Pauw, sheet resistance, RS, graphene, CVD graphene, four‑terminal, Ω/sq, SiO2 on Si, silicon carbide, 4PP, measurement uncertainty.
Технические детали
- Технический комитет
- TC 113 - Nanotechnology for electrotechnical products and systems
- SKU
- IEC TS 62607-6-7:2023
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